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0 3. Also purified from phenylsulfide impurities by dissolving in CHC13, washing with aq satd NaHC03, drying (Na2S04)evaporating and the residual oil was passed through a silica gel column (600g) and eluted with hexane-C6H6(lL, 4:1, eluting PhSSPh) then C6H6(1L) which elutes PhSSOZPh. High-speed conversion requires the use of a high-frequency clock.
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